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Characterizing thin-film adjustable X-ray optics using optical interferometry
Dissertation   Open access

Characterizing thin-film adjustable X-ray optics using optical interferometry

Kenneth Buffo
University of Iowa
Doctor of Philosophy (PhD), University of Iowa
Autumn 2025
DOI: 10.25820/etd.008191
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Abstract

X-ray observatories are critical for studying a myriad of high-energy sources (0.1 – 10keV) in the Universe: black holes, hot plasma surrounding galaxies, and the atmospheres of stars. In particular, several proposed X-ray missions will require thin (≤ 0.5 mm thick) mirrors with precise surface figures to maintain high angular resolution (≤ 0.5 arcsec). The development of thin X-ray mirrors enables increased effective areas in observatories, boosting their sensitivity for photon focusing. Mirrors that also have increased angular resolution enable observatories to distinguish closely spaced features in the sky, an essential attribute when observing sources at high redshifts. Similarly, synchrotron radiation sources rely on exquisite optics to probe materials at an unprecedented scale. Such optics are used to focus and shape X-ray beamlines by achieving strict surface height deviations (< 0.5 nm). This thesis is motivated by the need to develop state of the art X-ray optics to meet the technical requirements of future missions and facilities. One solution is to develop adjustable X-ray optics (AXROs). AXROs apply a thin film (1.5 – 2 μm thick) of high-actuation authority piezoelectric material deposited to their non-reflective side that is subsequently segmented to create an array of discrete actuators. When supplied an electric field, the film exhibits the converse piezoelectric effect creating a local figure change to the surface of the mirror. The deterministic control of AXRO actuators improves mirror figure quality to compensate for errors introduced during mirror fabrication, mounting, and changes in thermal environment. Thus, the primary goal of this dissertation is to mature the readiness of AXROs. This was accomplished by using optical interferometry to measure the surface of AXROs with great precision. More specifically, interferometry was used to measure actuator responses from a curved AXRO using lead zirconate titanate (PZT) after which the measured responses were used to characterize the figure correction capability and angular resolution improvement of the AXRO. Measurements were also made to calculate the stress induced from fabricating AXROs using a poly(vinylidene fluoride-trifluoroethylene) piezoelectric. Finally, the actuator performance of a flat AXRO using a PZT film was characterized for use in synchrotron sources.
Interferometry Physics adjustable optics metrology thin-film piezoelectric X-rays

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