A trans-1,2-diarylhexafluorocyclobutane

Dale C Swenson; Michiharu Yamomoto; Donald J Burton

doi:10.1107/S0108270197003764

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Journal article

Peer reviewed

A trans-1,2-diarylhexafluorocyclobutane

Dale C Swenson, Michiharu Yamomoto and Donald J Burton

Acta crystallographica. Section C, Crystal structure communications, Vol.53(10), pp.1445-1447

10/15/1997

DOI: 10.1107/S0108270197003764

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Abstract

Crystal structure analysis establishes the configuration of one of two isomers of the thermal dimerization of N-[3-(1,2,2-trifluoroethenyl)-4-phenoxyphenyl]phthalimide to be trans-5,5'-[1,2,3,3,4,4-hexafluorocyclobutane-1,2-diylbis(2-phenoxyphenyl)]-N,N'-bis(phthalimide), C44H24F6N2O6. The cyclobutane ring puckers and has a dihedral angle of 23.5 (4)°. The crystal also contains a diethyl ether molecule of solvation, C4H10O.

Physics

Condensed matter: structure, mechanical and thermal properties

Exact sciences and technology

Heterocyclic compounds

Organic compounds

Structure of solids and liquids; crystallography

Structure of specific crystalline solids

Details

Title: Subtitle: A trans-1,2-diarylhexafluorocyclobutane
Creators: Dale C Swenson - University of Iowa
Michiharu Yamomoto - Department of Chemistry, University of Iowa, Iowa City, IA 52242, United States
Donald J Burton - Department of Chemistry, University of Iowa, Iowa City, IA 52242, United States
Resource Type: Journal article
Publication Details: Acta crystallographica. Section C, Crystal structure communications, Vol.53(10), pp.1445-1447
Publisher: Blackwell
DOI: 10.1107/S0108270197003764
ISSN: 0108-2701
eISSN: 1600-5759
Language: English
Date published: 10/15/1997
Academic Unit: Chemistry
Record Identifier: 9984622749602771

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