Association of solvents improves selected properties of experimental dental adhesives

Francisbênia Alves Silvestre; Vitaliano Gomes de Araújo Neto; Marcelo Giannini; Tainah Oliveira Rifane; Karen Evellin Moura Cordeiro; Samara Tabata Cavalcante Braga Medeiros; Diego Lomonaco; Madiana Magalhães Moreira; Adyson Herbert Correia Alves; Victor Pinheiro Feitosa

doi:10.1590/1807-3107bor-2022.vol36.0093

Back

Association of solvents improves selected properties of experimental dental adhesives

Journal article

Open access

Peer reviewed

Association of solvents improves selected properties of experimental dental adhesives

Francisbênia Alves Silvestre, Vitaliano Gomes de Araújo Neto, Marcelo Giannini, Tainah Oliveira Rifane, Karen Evellin Moura Cordeiro, Samara Tabata Cavalcante Braga Medeiros, Diego Lomonaco, Madiana Magalhães Moreira, Adyson Herbert Correia Alves and Victor Pinheiro Feitosa

Brazilian oral research, Vol.36, pp.e093-e093

01/01/2022

DOI: 10.1590/1807-3107bor-2022.vol36.0093

PMID: 35830119

Files and links (1)

url

https://doi.org/10.1590/1807-3107bor-2022.vol36.0093View

Published (Version of record) Open Access

Abstract

The aim of the study was to evaluate how the association of solvents (tetrahydrofuran [THF], dimethyl sulfoxide [DMSO], ethanol [ET] or acetone [ACT]) with experimental dental adhesives affects selected properties of experimental dental adhesives and dentin bond durability. Six adhesive combinations were prepared containing: 30 % ET, 30 % ACT, 30 % THF, 28 % ET + 2 % DMSO (ET+DMSO), 15 % ethanol + 15 % THF (ET+THF), or 28 % THF + 2 % DMSO (THF+DMSO). Thirty-six molars (n = 6) were cut to expose the coronary dentin, and were randomly divided according to the adhesives. They were restored, and then cut into resindentin sticks (1 mm²), and stored in distilled water for 24 h or 6 months, until conducting the microtensile bond strength and nanoleakage tests. Other experiments performed with adhesives included viscosity assessment using a rheometer, and degree of conversion using Fourier-transform infrared spectroscopy (FTIR). The data were analyzed statistically using two-way ANOVA and Tukey's test (p < 0.05). The adhesive formulated exclusively with THF showed the highest viscosity, followed by ET+THF, which obtained the highest degree of conversion compared to ET, and THF alone. ET+DMSO obtained the highest 24-h and aged bond strengths (p < 0.05). ET+THF increased the nanoleakage slightly after 6 months, but attained the only gap-free adhesive interface among all the groups. The combination of alternative solvents, particularly THF, with conventional ones (ET) has improved chemical properties, and the dentin bonding of experimental simplified adhesives.

Dental Bonding - methods

Dentin

Dentin-Bonding Agents - chemistry

Dimethyl Sulfoxide

Ethanol

Materials Testing

Resin Cements - chemistry

Solvents - chemistry

Tensile Strength

Details

Title: Subtitle: Association of solvents improves selected properties of experimental dental adhesives
Creators: Francisbênia Alves Silvestre - Universidade de Fortaleza
Vitaliano Gomes de Araújo Neto - Universidade Estadual de Campinas (UNICAMP)
Marcelo Giannini - Universidade Estadual de Campinas (UNICAMP)
Tainah Oliveira Rifane - Universidade de Fortaleza
Karen Evellin Moura Cordeiro - Universidade de Fortaleza
Samara Tabata Cavalcante Braga Medeiros - Paulo Picanço School of Dentistry
Diego Lomonaco - Universidade Federal do Ceará
Madiana Magalhães Moreira - Universidade Federal do Ceará
Adyson Herbert Correia Alves - Universidade de Fortaleza
Victor Pinheiro Feitosa - Universidade de Fortaleza
Resource Type: Journal article
Publication Details: Brazilian oral research, Vol.36, pp.e093-e093
DOI: 10.1590/1807-3107bor-2022.vol36.0093
PMID: 35830119
NLM abbreviation: Braz Oral Res
ISSN: 1807-3107
eISSN: 1807-3107
Language: English
Date published: 01/01/2022
Academic Unit: Operative Dentistry
Record Identifier: 9984655345202771

Metrics

14 Record Views

1 Times Cited - Web of Science