Journal article
Crystal and molecular structure of [H3O·18-crown-6]2-[ReCl6] isolated from a liquid clathrate medium
Journal of chemical crystallography, Vol.26(1), pp.59-61
01/1996
DOI: 10.1007/BF02018698
Abstract
The crystal and molecular structure of [H3O·18-crown-6]2[ReCl6] 1 is reported. Crystal data for 1: trigonal, space group R 3, a = 13.857(2) Å, c = 10.154(2) Å, Dc = 2.85 g/cm3, Z = 3, Rf = 0.073, Rw = 0.064. The oxonium ion is observed to be crystallographically disordered lying 0.37 Å on both sides of the plane defined by the crown ether oxygen atoms. The anion resides on a crystallographic 3 position forming a slightly distorted octahedron.
Details
- Title: Subtitle
- Crystal and molecular structure of [H3O·18-crown-6]2-[ReCl6] isolated from a liquid clathrate medium
- Creators
- Leonard J BarbourLeonard R MacGillivrayJerry L Atwood
- Resource Type
- Journal article
- Publication Details
- Journal of chemical crystallography, Vol.26(1), pp.59-61
- DOI
- 10.1007/BF02018698
- ISSN
- 1074-1542
- eISSN
- 1572-8854
- Language
- English
- Date published
- 01/1996
- Academic Unit
- Chemistry; Pharmaceutical Sciences and Experimental Therapeutics
- Record Identifier
- 9984216723602771
Metrics
3 Record Views