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Determination of crystallographic orientation of large grain metals with surface acoustic waves
Journal article   Open access   Peer reviewed

Determination of crystallographic orientation of large grain metals with surface acoustic waves

Wenqi Li, Steve D Sharples, Richard J Smith, Matt Clark and Michael G Somekh
The Journal of the Acoustical Society of America, Vol.132(2), pp.738-745
08/2012
DOI: 10.1121/1.4731226
PMID: 22894196
url
https://nottingham-repository.worktribe.com/output/3156906View
Open Access

Abstract

A previously described laser ultrasonic technique known as spatially resolved acoustic spectroscopy (SRAS) can be used to image surface microstructure, using the local surface acoustic wave (SAW) velocity as a contrast mechanism. It is shown here that measuring the SAW velocity in multiple directions can be used to determine the crystallographic orientation of grains. The orientations are determined by fitting experimentally measured velocities to theoretical velocities. Using this technique the orientations of 12 nickel and 3 aluminum single crystal samples have been measured, and these are compared with x-ray Laue backreflection (LBR) measurements with good agreement. The root mean square difference between SRAS and LBR measurements in terms of an R-value is less than 4.1°. The influence of systematic errors in the SAW velocity determination due to instrument miscalibration, which affects the accurate determination of the planes, is discussed. SRAS has great potential for complementary measurements or even for replacing established orientation determination and imaging techniques.
Motion Reproducibility of Results Aluminum - chemistry Models, Chemical Nickel - chemistry Elasticity Crystallography, X-Ray Calibration Spectrum Analysis - standards Spectrum Analysis - instrumentation Lasers Surface Properties Ultrasonics - instrumentation Molecular Structure Crystallography - instrumentation Ultrasonics - standards Crystallography - standards

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