Journal article
Preparative purification of a high-mannose type N-glycan from soy bean agglutinin by hydrazinolysis and tyrosinamide derivatization
Analytical biochemistry, Vol.265(2), pp.313-316
12/15/1998
DOI: 10.1006/abio.1998.2895
PMID: 9882408
Abstract
The N-linked oligosaccharide from soy bean agglutinin (Man9) was isolated on a preparative scale following derivatization with Boc-tyrosine. The procedure utilized preparative hydrazinolysis to release the oligosaccharide and yielded multi-micromol quantities of Boc-tyrosine-Man9 which was characterized by 1H NMR and ES-MS.
Details
- Title: Subtitle
- Preparative purification of a high-mannose type N-glycan from soy bean agglutinin by hydrazinolysis and tyrosinamide derivatization
- Creators
- David L Evers - Division of Medicinal Chemistry and Division of Pharmaceutics, College of Pharmacy, University of Michigan, 428 Church Street, Ann Arbor, Michigan, 48109-1065, USARex L HungV Hayden ThomasKevin G Rice
- Resource Type
- Journal article
- Publication Details
- Analytical biochemistry, Vol.265(2), pp.313-316
- DOI
- 10.1006/abio.1998.2895
- PMID
- 9882408
- NLM abbreviation
- Anal Biochem
- ISSN
- 0003-2697
- eISSN
- 1096-0309
- Publisher
- United States
- Grant note
- GM07767 / NIGMS NIH HHS GM48049 / NIGMS NIH HHS
- Language
- English
- Date published
- 12/15/1998
- Academic Unit
- Pharmaceutical Sciences and Experimental Therapeutics; Craniofacial Anomalies Research Center; Medicinal and Natural Products Chemistry
- Record Identifier
- 9984065310102771
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