Journal article
Quantification of 13C in solids using CPMAS-DD-NMR spectroscopy
Analytica chimica acta, Vol.283(3), pp.1033-1043
1993
DOI: 10.1016/0003-2670(93)80264-L
Abstract
Quantitative analysis of several standard materials is used to evaluate various techniques for analysis of
13C cross polarization magic angle spinning dipolar decoupling (CPMAS-DD)-NMR spectra. These results suggest that uncertainty in the kinetics of the initial cross-polarization process may lead to systematic errors in the fitting of CPMAS-DD-NMR data. Methods are suggested to minimize the effects of this potential source of error. These results indicate that
13C CPMAS-DD-NMR can give quantitatively reliable results.
Details
- Title: Subtitle
- Quantification of 13C in solids using CPMAS-DD-NMR spectroscopy
- Creators
- David G Rethwisch - Department of Chemical and Biochemical Engineering, University of Iowa, Iowa City, IA 52242 USAMary A JacinthaCecil R Dybowski
- Resource Type
- Journal article
- Publication Details
- Analytica chimica acta, Vol.283(3), pp.1033-1043
- Publisher
- Elsevier B.V
- DOI
- 10.1016/0003-2670(93)80264-L
- ISSN
- 0003-2670
- eISSN
- 1873-4324
- Language
- English
- Date published
- 1993
- Academic Unit
- Chemical and Biochemical Engineering
- Record Identifier
- 9984003451502771
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